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ASTM D4294-16e1

ASTM D4294-16e1

Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry

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1.1 ,This test method covers the determination of total sulfur in petroleum and petroleum products that are single-phase and either liquid at ambient conditions, liquefiable with moderate heat, or soluble in hydrocarbon solvents. These materials can include diesel fuel, jet fuel, kerosine, other distillate oil, naphtha, residual oil, lubricating base oil, hydraulic oil, crude oil, unleaded gasoline, gasoline-ethanol blends, biodiesel (see Note 2), and similar petroleum products.

Note 1: ,Oxygenated fuels with ethanol or methanol contents exceeding the limits given in Table 1 can be dealt with using this test method, but the precision and bias statements do not apply (see Appendix X3).

(A) ,The concentrations of substances in this table were determined by the calculation of the sum of the mass absorption coefficients times mass fraction of each element present. This calculation was made for dilutions of representative samples containing approximately 3 ,% of interfering substances and 0.5 ,% sulfur.

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