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ASTM D7303-17 + Redline

ASTM D7303-17 + Redline

Standard Test Method for Determination of Metals in Lubricating Greases by Inductively Coupled Plasma Atomic Emission Spectrometry

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1.1 ,This test method covers the determination of a number of metals such as aluminum, antimony, barium, calcium, iron, lithium, magnesium, molybdenum, phosphorus, silicon, sodium, sulfur, and zinc in unused lubricating greases by inductively coupled plasma atomic emission spectrometry (ICP-AES) technique.

1.1.1 ,The range of applicability for this test method, based on the interlaboratory study conducted in 2005,2 is aluminum (10 to 600), antimony (10 to 2300), barium (50 to 800), calcium (20 to 50 ,000), iron (10 to 360), lithium (300 to 3200), magnesium (30 to 10 ,000), molybdenum (50 to 22 ,000), phosphorus (50 to 2000), silicon (10 to 15 ,000), sodium (30 to 1500), sulfur (1600 to 28 ,000), and zinc (300 to 2200), all in mg/kg. Lower levels of elements may be determined by using larger sample weights, and higher levels of elements may be determined by using smaller amounts of sample or by using a larger dilution factor after sample dissolution. However, the test precision in such cases has not been determined, and may be different than the ones given in Table 1.

TABLE 1 Precision of Grease Analysis

Note 1: ,X is the mean concentration in mg/kg.

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