1.1 ,This test method covers the determination of hydrogen in nuclear-grade mixed oxides of uranium and plutonium ((U, Pu)O2) sintered fuel pellets. This test method is an alternative to Test Method C698 for the determination of moisture in nuclear-grade sintered mixed oxide (MOX) fuel pellets. Test Method C698 describes the detection of moisture in mixed oxides using a coulometric, electrolytic moisture analyzer. Although the main source of H2 in the fuel pellets is moisture, there could be other sources. The MOX pellet Specification C833 specifies a limit for hydrogen from all sources, not only moisture. The inert gas fusion followed by thermal conductivity detector specified in this test method allows for detection of hydrogen from all sources. Therefore, this test method can be used to determine the limit specified in C833.